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On the several-min try (Fig. 3F), the massive diamond grain is the fundamental structure, because the confirmed by the inset FFT image of diamond (111) diffraction areas plus the Raman range inside the Quand Appendix, Fig. S5, that’s like the newest 0-min sample, guaranteeing the graphite provides entirely changed into diamond and you will shaped a bulk diamond amazingly compared to the first (2 to 4 min) and you will second time periods (5 to 9 min). These types of performance surely verify that the new blended look of diamond (111) and you may graphite (002) in the attempt 8-minute is an excellent transformation period away from graphite so you can diamond. Artificial diamond takes on a vital role regarding the development industry, jewelry, and you will upcoming photoelectronic gizmos, however it is a button difficulty to prepare the desired high-area diamonds.
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- The fresh 0-s try (Fig. 2A) displays higher pole-for example diamond crystals confirmed because of the diffraction spots on the diamond (111) positioning from the inset Fourier changes (FFT) picture.
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Concurrently, an excellent flake-such diamond crystal (reddish photo within the Fig. 2D-2) implies that diamond begins to are available, within the an excellent agreement on the SEM and you may Raman spectra. To the 120-s attempt, of a lot nanodiamond crystals nude for the side of cauliflower-including dirt safeguarded the new graphite nanorods (Fig. 2E-2). These performance show the new NCD characteristics present in the new Raman range.